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Laser-Induced Breakdown Spectroscopy for Determination of the Organic Oxygen Content in Anthracite Coal Under Atmospheric Conditions
Volume 62, Number 4 (April 2008) Page 458-463
Zhang, Lei; Dong, Lei; Dou, Haipeng; Yin, Wangbao; Jia, Suotang
Laser-induced breakdown spectroscopy has been used to measure the organic oxygen content in pulverized anthracite coal under atmospheric conditions. Special spectral processing including the optimal O(I) emission-line selection by comparing the spectral correlation coefficients with the N(I) line, internal normalization with the N(I) line, and temperature correction are proposed and employed to satisfy the multi-line analysis method and yield the most accurate quantitative results. The calibration method for determining the organic oxygen content of coal is presented, with an accuracy of 1.15-1.37% and an average relative error of 19.39% being evaluated through an experiment performed on six anthracite coal samples. The relative measurement error distribution has also been studied.