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Mass Spectral Analysis of Acid- and Base-Sensitive Alcohols as Phenylcarbamates

Volume 28, Number 2 (April 1974) Page 200-200

Rosen, R.T.; Durbetaki, A.J.; Alvarez, M.

The usual methods of derivatization of alcohols which are unstable in the mass spectrometer fail with those alcohols which are acid- and/or base-sensitive. Examples include the acid-sensitive acetal group and the acid- and base-sensitive oxirane ring, as in structures I and II, respectively.