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Simultaneous Analysis of Gas Phase and Intermediates in the Hydrogenation of Carbon Oxides by DRIFTS

Volume 47, Number 11 (Nov. 1993) Page 1760-1766

Benitez, J.J.; Carrizosa, I.; Odriozola, J.A.


In this work the experimental details and some examples of applications of diffuse reflectance infrared technique are described. Special interest has been devoted to a correct determination of the temperature of the sample, to gas-phase analysis, and to quantitative aspects in a DRIFTS controlled environmental cell. Applications to the analysis of the gas phase during catalytic hydrogenation and to the obtainment of kinetic parameters for the catalytic decomposition of adsorbates are included.